loss on drying we applied vaccum for some compounds and
some compounds are at 105c why
Answers were Sorted based on User's Feedback
Thermally liable compounds are dried in hot air oven.
Thermally un stable compounds are dried under vaccum.
Vaccum is applied to prevent sample loss due to
splashing,foming.Low boiling samples are dried under vaccum.
| Is This Answer Correct ? | 16 Yes | 1 No |
Answer / falguni
As per
PV=NRT, if we decrease pressure, temperature also decrease.
Vacuum i.e. no pressure. If we heat our sample which has
low melting point(near 60C), it melts at 60C. Vacuum lowers
the temprature but effect on sample is in equilibrum to the
higher temperature. It does not melt the sample but remove
volatile solvents and adsorbed water.
| Is This Answer Correct ? | 7 Yes | 0 No |
Answer / virender
In a Vacuum Oven, the thermal processes occur in an airtight
chamber where a desired level of vacuum has been applied
using an external vacuum pump (not included). With a vacuum
oven the entire application can take place under vacuum or a
controlled atmosphere can be created through the
introduction of an inert gas. Vacuum ovens can help in the
prevention of surface reactions (such as oxidation),
decontaminating samples (removing lubricants for example) as
well as for speeding up the out gassing process. When
determining the process you will use for a vacuum oven bear
in mind that you will need to size a pump to meet this
application. This requires defining the appropriate chamber
size, the level of vacuum desired, and how quickly you will
need to reach that desired vacuum level.
| Is This Answer Correct ? | 2 Yes | 0 No |
what is the use of tap density apparatus? why we calculate it? what is the difference between the bulk density and tap density?
1 Answers Alchemist, Alembic, Apex,
what is custom fields in waters system?
1 Answers Akorn India, Aurobindo,
Why sulpuric acid only used to ROI but not used nitric acid and some other acids?
7 Answers Cadila, Laurus, Ranbaxy,
What is the purpose & importance of using the polystyrene film in ir calibration?
what are the guidelines for analytical method validations?
Why do we use 0.005M h2so4 solution for preparation of k2cr2o7 solution for UV calibration?
3 Answers Jubilant, Medreich, Mylan,
What is method validation in quality control
Why are using in Hi,zero air, Ni gass are used GC
5 Answers Aurobindo, ELBS, Vimta Labs,
why we use holmiumperchlorate in calibrating uv
4 Answers Aurobindo, DRL, MSN Pharma,
What is the difference between Capillary column and Packed column.
7 Answers Cipla, Hetero, Sun Pharma, Supreme Petrochem,
why we do the calibration of limit of stry light in hplc & uv
why we are calibrating autopolarimeter with quartz control plates