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how do u optimise hplc method
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Hello Dear all; I have a technical question related to analytical Chemistry, I have a sample of (40% w/w) Ferric Chloride solution (for water treatment purposes which consist a little portions of Ferrous Chloride and Hydrochloric acid. I need to know the methods to determine the percentages of each Ferrous Chloride and Chloride acid. Also I want to make sure that this solution is truly (40% w/w). So ANY CLUE !!! Thanks in advance.
My question about gas chromatography sulfur chemiluminsecence detector. I test unknown sample gas by GC-SCD (calibrated ) and the result of *H2S is 279 PPM , *but when I test the same sample with the GC-TCD (calibrated ) the value of *H2S is 2500 PPM . I'd like to inform you that both GCs are calibrated and have very good operation conditions with stable parameters . the question is if the sample gas with higher H2S over detection limits of SCD detector (1000 ppm). why the result it 279 ppm Best regards
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2 Answers GMP Pharma, Optimus,
Organic Chemistry 
