How to Perform a Recrystallization ?
Answers were Sorted based on User's Feedback
Answer / taksena gurung
1 First choose a proper solvent to dissolve the impure
substance. the solvent should be like that, in cold
condition the substance is insoluble or partially soluble,
and in hot condition the substance should be completely
soluble.
2 After selecting the suitable solvent, dissolve the given
substance in it, and heat it till the substance completly
dissolve forming clear solution.
3 now filter this hot solution immediatly through the
filter paper. the insoluble impurity remains on the filter
paper and collect the filtrate in a dish and allow to cool
without disturbng the container.
4 the filtrate on cooling gives crystals which are pure,
homogenous, and bigger in size.
| Is This Answer Correct ? | 33 Yes | 0 No |
Answer / bhavin mehta
Recrystallization is a laboratory technique used to purify
solids based on their different solubilities.
Recrystallization Steps are
1)Add a small quantity of appropriate solvent to an impure
solid.
2)Apply heat to dissolve the solid.
3)Cool the solution to crystallize the product.
4)Use vacuum fitration to isolate and dry the purified
solid.
| Is This Answer Correct ? | 10 Yes | 5 No |
Answer / dinesh gurav
Recrystallisation is a crystallisation process of impure or
crude solid materials in different solvents and at diff.
experimental parameters like temp,pH and quantity of
solvents to elute out the unwanted compounds
[Impurities,Polymorphs] to get a compound of desired
quality.
| Is This Answer Correct ? | 4 Yes | 2 No |
Answer / tulasi
if compoune is dissolved in acid
then we have to add base and viceversa
| Is This Answer Correct ? | 1 Yes | 9 No |
In which situation we require to prepare the standard solution from sample in Related substance method?
WHY KBr is used in IR Spectroscopy
why we use glass fiber filters use in some situation?
how to select short coloum and long coloumn for new molecule
Why used 0.02% v/v solution of toluene in hexane for calibration of UV.
What is the principle of HPLC, GC, LCMS, GCMS,LC QQQ, GC QQQ, LC Q TOF and GC Q TOF. What are the applications and Specificity?
How can we confirm the HPLC column is end-capped or not? Is it possible to identify by physical appearance?
in OSD forms require to use gas chromatography?
What is the acceptance criteria for moisture balance when calibrated with sodium sulfate
Is there any difference in principal of reverse phase and normal phase chromatography? and why? Please update. Thank and regard
what is the meaning of linearity,principle of co-relation coefficient?
why RID detector is used for selective materials like Mannitol, Hydroxyethyl Starch and Sorbitol?