How to Perform a Recrystallization ?

Answer Posted / taksena gurung

1 First choose a proper solvent to dissolve the impure
substance. the solvent should be like that, in cold
condition the substance is insoluble or partially soluble,
and in hot condition the substance should be completely
soluble.
2 After selecting the suitable solvent, dissolve the given
substance in it, and heat it till the substance completly
dissolve forming clear solution.
3 now filter this hot solution immediatly through the
filter paper. the insoluble impurity remains on the filter
paper and collect the filtrate in a dish and allow to cool
without disturbng the container.
4 the filtrate on cooling gives crystals which are pure,
homogenous, and bigger in size.

Is This Answer Correct ?    32 Yes 0 No



Post New Answer       View All Answers


Please Help Members By Posting Answers For Below Questions

cefoperozone and sulbactam inj. hplc test method

2125


how you determine moist.of NaOH sol or NaOH flacks

1768


In HPLC calibration, caffeine is used as primary standard for wave length calibration due to caffeine is having dual maxima at 273 & 205 nm and one minima at 245 nm. Any body can give reference of these details from any pharmacopeia (with chapter no.) or any other authentic guideline?

1451


What is the requirement for brazil in the analytical method vslidation comparr to ich?

270


which are the sizes of capsules?

402






inhouse product is in capsule form in combination and RLD is in tablet form then can we proceed for multimedia CDP? in inhouse capsule product disso is paddle with sinker in release media is there then RLD product in tablet form then with same as paddle with sinker we can proceed n.a.?

289


How to set analytical specification for combination products?

324


please explian me about area normalisation method,diluted standard method,impurity vs impurity and which one has to be selected in method development

1098


WHAT IS THE CRITERIA FOR SELECTION OF TIME OF DISSOLUTION AND THE MEDIUM OF DISSOLUTION?

2138


how require to interprit the method precision data of hptlc?

294


Why six unit used for precision?

798


CAN WE DETERMINE THE PEAK PURITY IN GAS CHROMATOGRAPHY ANALYSIS?

701


How much is the standard area for glc analysis

1744


Why we select scan range from higer wavelength to lower wavelength in uv visible spectroscopy and ftir spectroscopy ? .

456


what is diffrence between specificity and selecivity?

306