A column is said to be endcapped when a small silylating
agent (e.g., trimethylchlorosilane) is used to bond residual
silanol groups on a packing surface.
As per LOD at higher temperature we identify the total volatile substances including water. LOD at lower temperature (60°C to 70°C)under vacuum we can't identify the water, then we will fined water through K.F reagent