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what is the defination of calibration & verification?

Answer Posted / pankaj pawar

Calibration is simply the process of comparing the unknown with a reference standard and reporting the results. For example:
Applied= 1.30V, Indicated= 1.26V (or Error= -0.04V)
Calibration may include adjustment to correct any deviation from the value of the standard.

Verification, as it relates to calibration, is the comparison of the results against a specification, usually the manufacturer's published performance figures for the product. (e.g. Error= -0.04V, Spec= ±0.03V, "FAIL"). Some cal labs include a spec status statement on their Certificate of Calibration. (i.e. the item did/did not comply with a particular spec).

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My question about gas chromatography sulfur chemiluminsecence detector. I test unknown sample gas by GC-SCD (calibrated ) and the result of *H2S is 279 PPM , *but when I test the same sample with the GC-TCD (calibrated ) the value of *H2S is 2500 PPM . I'd like to inform you that both GCs are calibrated and have very good operation conditions with stable parameters . the question is if the sample gas with higher H2S over detection limits of SCD detector (1000 ppm). why the result it 279 ppm Best regards

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